Data collection and processing statistics
| Crystal . | F8_w (cross-linked) . | Nat-7 . | Nat-4b . | Nat-4c . |
|---|---|---|---|---|
| Wavelength, Å | 1.0246 | 1.00 | 1.00 | 1.00 |
| Unit cell, Å | a = b = 134.7, c = 353.6 | a = b = 134.5, c = 359.7 | a = b = 134.6, c = 359.5 | a = b = 134.8, c = 358.4 |
| Resolution, Å | 30-4.5 (4.6-4.5) | 100-4.3 (4.4-4.3) | 100-3.9 (4.0-3.9) | 100-3.7 (3.76-3.70) |
| No. reflections (no. unique reflections) | 308 594 (20 241) | 133 617 (42 517) | 199 559 (28 509) | 189 184 (34 208) |
| Redundancy | 15.2 | 3.1 | 7.0 (2.9) | 5.5 (3.0) |
| I/σ (I)* | 19.5 (5.4) | 17.7 (3.5) | 12.9 (1.0) | 13.7 (0.91) |
| Completeness, %* | 100 (100) | 97.7 (98.6) | 92.5 (61.3) | 94.5 (67.3) |
| Rsym* | 0.161 (0.682) | 0.084 (0.553) | 0.092 (0.735) | 0.096 (0.798) |
| Crystal . | F8_w (cross-linked) . | Nat-7 . | Nat-4b . | Nat-4c . |
|---|---|---|---|---|
| Wavelength, Å | 1.0246 | 1.00 | 1.00 | 1.00 |
| Unit cell, Å | a = b = 134.7, c = 353.6 | a = b = 134.5, c = 359.7 | a = b = 134.6, c = 359.5 | a = b = 134.8, c = 358.4 |
| Resolution, Å | 30-4.5 (4.6-4.5) | 100-4.3 (4.4-4.3) | 100-3.9 (4.0-3.9) | 100-3.7 (3.76-3.70) |
| No. reflections (no. unique reflections) | 308 594 (20 241) | 133 617 (42 517) | 199 559 (28 509) | 189 184 (34 208) |
| Redundancy | 15.2 | 3.1 | 7.0 (2.9) | 5.5 (3.0) |
| I/σ (I)* | 19.5 (5.4) | 17.7 (3.5) | 12.9 (1.0) | 13.7 (0.91) |
| Completeness, %* | 100 (100) | 97.7 (98.6) | 92.5 (61.3) | 94.5 (67.3) |
| Rsym* | 0.161 (0.682) | 0.084 (0.553) | 0.092 (0.735) | 0.096 (0.798) |
Space group is P41212.
Numbers in parentheses are statistics from the highest-resolution shells.